Biosynthesis of TiO2 nanoparticles using red seaweed: Detailed characterization

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Research Paper 06/03/2025
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Biosynthesis of TiO2 nanoparticles using red seaweed: Detailed characterization

Swapnil B. Patil, D. B. Nakade
Int. J. Biosci.26( 3), 36-45, March 2025.
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Abstract

This research presents the green synthesis of titanium dioxide (TiO) nanoparticles (NPs) using red seaweed extract and their comprehensive characterization through various analytical techniques. The synthesis process yielded spherical and crystalline TiO NPs with sizes ranging from 93.20 to 110.5 nm. Characterization was performed using SEM, TEM, FTIR, XRD, DLS, and AFM analyses. SEM and TEM revealed highly crystalline structures with well-defined lattice fringes, confirming their suitability for photocatalytic applications. FTIR analysis indicated the presence of organic residues and the successful formation of TiO. XRD analysis identified prominent peaks corresponding to anatase and rutile phases, with minor indications of brookite phase or impurities. DLS measurements showed a Z-average diameter of 114 nm with a moderately broad size distribution (PDI of 0.34). AFM analysis highlighted the moderately rough surface and high surface area, enhancing photocatalytic efficiency. This study underscores the potential of red seaweed extract-mediated synthesis as a green, sustainable method for producing TiO NPs with promising photocatalytic properties, suggesting further optimization for enhanced applications in environmental remediation and antimicrobial treatments.

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