Oxymatrine degradation in cucumber fruit, leaves, and soil in Iraq

Paper Details

Research Paper 01/10/2018
Views (436) Download (26)
current_issue_feature_image
publication_file

Oxymatrine degradation in cucumber fruit, leaves, and soil in Iraq

Hussain A. Hussain, Abdul kareem Jawad Ali, Saleh Hassan Sumir
J. Bio. Env. Sci.13( 4), 38-44, October 2018.
Certificate: JBES 2018 [Generate Certificate]

Abstract

This experiment was conducted in the National Centre for Pesticides Control (NCPC)/Ministry of Agriculture during winter season 2017-2018 Toknow the degredation of Oxymatrine in cucumber fruit ,leaves and soil in greenhouse and the period of this degradation  and pre harvest interval for consumers and to know the range of appropriateness the new method of extraction with cucumber, the High performances Liquid Chromatography (HPLC) was employed as analyses equipment and QuEChERS (Quick, Easy, Cheap, Effective, Rugged and Safe) approaches as extraction method. The obtained results were showed that Oxymatrine in cucumber fruit, leaves, and green house  soil  degradation was acquired in 5th, 7th, and 2th day respectively after the treatment ,then the hplc system did not detected any quantity from the insecticide oxymatrine, 7 day is the pre harvest interval(PHI),The  average recoveries of   Oxymatrine in cucumber  fruit and leaves  was  84-86.2%, in soil was 102.3-102.9%, with the relative standard deviation (RSD) 1.1% and 0.9%  respectively. Through the results of this achievement, we determing the safety holding periods before the process of fruits reaping which was impossible to predict because the Oxymatrine does not have MRL in the Codex Alimentarius and European Union guideline and United States Environmental Protection Agency (USEPA), and the range of appropriateness the new method of extraction with cucumber as a future study we will expand the study of the degradation of Oxymatrine on other agricultural crops in the food basket for the Iraqi consumer.

VIEWS 61

Huang S, Li R, Zhang Z, Li L, Gu X, Fan W, Lucas WJ, Wang X, Xie B, Ni P, Ren Y. 2009. The genome of the cucumber, Cucumis sativus L. Nature genetics, 41(12), p 1275.

Anton R, Patri F, Silano V. 2001. Plants in cosmetics: Plants and plant preparations used as ingredients for cosmetic products. Volume II. Council of Europe Publishing.

Abu-Reidah I, Arráez-Román D, Quirantes-Piné R, Fernández-Arroyo S, Segura-Carretero A, Fernández-Gutiérrez A. 2012. HPLC–ESI-Q-TOF-MS for a comprehensive characterization of bioactive phenolic compounds in cucumber whole fruit extract. Food Research International. 46, 108-117.

Gholami Z, Sadeghi A. 2016. Management Strategies for Western Flower Thrips in Vegetable Greenhouses in Iran: a Review. Plant Protect. Sci. 52(2), 87-98.

Liu G, Dong J, Wang H, Hashi Y, Chen S. 2011. Characterization of alkaloids in Sophora flavescens Ait. by high-performance liquid chromatography–electrospray ionization tandem mass spectrometry. Journal of pharmaceutical and biomedical analysis 54(5), p 1065-1072.

Lim SJ, Jeong DY, Choi GH, Park BJ, Kim JH. 2014. Quantitative analysis of matrine and oxymatrine in Sophora flavescens extract and its biopesticides by UPLC. Journal of Agricultural Chemistry and Environment 3(02), p.64.

Sineria company  Ltd.cyprus. 2016. Levo 2.4 S.L. www.sineria.org.

Rabea EI, Nasr HM, Badawy MEI. 2010. Toxic Effect and Biochemical Study of Chlorfl uazuron, Oxymatrine, and Spinosad on Honey Bees (Apis mellifera). Arch. Environ. Contam. Toxicol, 58, 722-732.

Anastassiades M, Lehotay SJ, Štajnbaher D. Schenck FJ. 2003. Fast and easy multiresidue method employing acetonitrile extraction/ partitioning and “dispersive solid-phase extraction” for the determination of pesticide residues in produce. Journal of AOAC international 86(2), p 412-431.