Tumor suppressing ability of myrtenal in DMBA-induced rat mammary cancer: A biochemical and histopathological evaluation

Paper Details

Research Paper 13/08/2025
Views (4)
current_issue_feature_image
publication_file

Tumor suppressing ability of myrtenal in DMBA-induced rat mammary cancer: A biochemical and histopathological evaluation

Manoharan Pethanasamy, Shanmugam M. Sivasankaran, Saravanan Surya, Raju Kowsalya
Int. J. Biosci. 27(2), 141-150, August 2025.
Copyright Statement: Copyright 2025; The Author(s).
License: CC BY-NC 4.0

Abstract

Breast cancer is one of the most common cancers in women and a major cause of deaths. 7,12-Dimethylbenz(a)anthracene (DMBA) is often used to induce breast cancer in rats. This study investigates the potential of myrtenal to prevent breast cancer caused by DMBA in female Sprague-Dawley rats. This study evaluates the dose-dependent chemopreventive effect of myrtenal in female Sprague-Dawley rats with mammary tumors induced by 7,12-dimethylbenz[a]anthracene (DMBA). The subcutaneous injection of DMBA alone in rats resulted in 100% tumor incidence accompanied by an increase in tumor burden, volume, and significant biochemical disruptions. Myrtenal at doses of 100, 200, and 400 mg/kg was orally administered to DMBA-treated rats, and its protective efficacy was evaluated through tumor inhibition potential, histopathological, and biochemical analyses. Myrtenal treatment caused a dose-dependent reduction in tumor incidence and volume and restored altered biochemical parameters (lipid peroxidation byproducts, antioxidants, and phase I and II detoxifying enzymes) toward normal. Histopathological findings further validated the protective effects of myrtenal. This study highlights the potent chemopreventive potential of myrtenal, particularly at 400 mg/kg. Myrtenal’s anticancer efficacy is primarily attributed to its strong antioxidant properties and its regulatory influence on the detoxification pathway.

Adelegan AA, Talabi AA, Dokunmu TM, Iweala EEJ. 2024. Anticancer activity of ethyl acetate fraction and ethanol leaf extract of Olax subscorpioidea against DMBA-induced female rats. Tropical Journal Natural Product Research 8(1), 6039-6044. https://doi.org/10.26538/tjnpr/v8i1.47.

Al Kury LT, Abdoh A, Ikbariah K, Sadek B, Mahgoub M. 2021. In Vitro and In Vivo Antidiabetic Potential of Monoterpenoids: An Update. Molecules 27(1), 182. https://doi.org/10.3390/molecules27010182

Basak D, Uddin MN, Hancock J. 2020. The Role of Oxidative Stress and Its Counteractive Utility in Colorectal Cancer (CRC). Cancers (Basel) 12(11), 3336. https://doi.org/10.3390/cancers12113336

Beutler E, Kelly BM. 1963. The effect of sodium nitrite on red cell GSH. Experientia 19, 96-97. https://doi.org/10.1007/BF02148042

Boopathy LK, Roy A, Gopal T, Kandy RRK, Arumugam MK. 2024. Potential molecular mechanisms of myrtenal against colon cancer: A systematic review. Journal of  Biochemical and  Molecular Toxicology 38(1), e23525. https://doi.org/10.1002/jbt.23525.

Booupathy LK, Venkatachalam S, Natarajan N, Thamaraiselvan R, Arumugam M, Periyasamy BM. 2016. Chemopreventive effect of myrtenal on bacterial enzyme activity and the development of 1,2-dimethyl hydrazine-induced aberrant crypt foci in Wistar Rats. Journal of Food and Drug Analysis 1, 206-213.  https://doi.org/10.1016/j.jfda.2015.07.003.

Buddhan R, Manoharan S, Naidu RM, Karthik M, Neelakandan M. 2020. Chemopreventive potential of myrtenal in 7,12-dimethylbenz(a)anthracene induced experimental oral carcinogenesis in golden Syrian hamsters. Journal of Clinical and Diagnosis Research 14(4), XC01-XC06. https://doi.org/10.7860/JCDR/2020/43399.13644

Burguin A, Diorio C, Durocher F. 2021. Breast Cancer Treatments: Updates and New Challenges. Journal of Personalized Medicine 11(8), 808. https://doi.org/10.3390/jpm11080808.

Carlberg I, Mannervik B. 1985. Glutathione reductase. Methods in Enzymology 113, 484-90. https://doi.org/10.1016/s0076-6879(85)13062-4.

Costa I, Solanas M, Escrich E. 2002. Histopathologic characterization of mammary neoplastic lesions induced with 7,12 dimethylbenz(alpha)anthracene in the rat: a comparative analysis with human breast tumors. Archives of Pathology & Laboratory Medicine 126(8), 915-927. https://doi.org/10.5858/2002-126-0915-HCOMNL

Desai ID. Vitamin E analysis methods for animal tissues. 1984. Methods in Enzymology 105, 138-147.https://doi.org/10.1016/s0076-6879(84)05019-9.

Di Carlo E, Sorrentino C. 2024. Oxidative Stress and Age-Related Tumors. Antioxidants (Basel) 13(9), 1109.https://doi.org/10.3390/antiox13091109

Dong R, Wang J, Guan R, Sun J, Jin P, Shen J. 2025. Role of Oxidative Stress in the Occurrence, Development, and Treatment of Breast Cancer. Antioxidants (Basel) 14(1), 104. https://doi.org/10.3390/antiox14010104.

Dragomanova S, Andonova V, Volcho K, Salakhutdinov N, Kalfin R, Tancheva L. 2023. Therapeutic Potential of Myrtenal and Its Derivatives-A Review. Life (Basel) 13(10), 2086. https://doi.org/10.3390/life13102086.

Ernster L. 1958. Diaphorase activities in liver cytoplasmic fractions. Federation Proceedings 17(1), 9650.

Habig WH, Pabst MJ, Jakoby WB. 1974. Glutathione S-transferases. The first enzymatic step in mercapturic acid formation. Journal of Biological Chemistry 249(22), 7130-7139.

Hari Babu L, Perumal S, Balasubramanian MP. 2012. Myrtenal attenuates diethylnitrosamine-induced hepatocellular carcinoma in rats by stabilizing intrinsic antioxidants and modulating apoptotic and anti-apoptotic cascades. Cellular Oncology (Dordrecht) 35(4), 269-283. https://doi.org/10.1007/s13402-012-0086-4.

Hollern DP, Swiatnicki MR, Andrechek ER. 2018. Histological subtypes of mouse mammary tumors reveal conserved relationships to human cancers. PLoS Genetics 14(1), e1007135. https://doi.org/10.1371/journal.pgen.1007135

Iacopetta D, Ceramella J, Catalano A, Scali E, Scumaci D, Pellegrino M, Aquaro S, Saturnino C, Sinicropi MS. 2023. Impact of cytochrome P450 enzymes on the phase I metabolism of drugs. Applied Sciences 13(10), 6045. https://doi.org/10.3390/app13106045.

Jena AB, Samal RR, Bhol NK, Duttaroy AK. 2023. Cellular Red-Ox system in health and disease: The latest update. Biomedicne and Pharmacotherapy 162, 114606.  https://doi.org/10.1016/j.biopha.2023.114606.

Jomova K, Raptova R, Alomar SY, Alwasel SH, Nepovimova E, Kuca K, Valko M. 2023. Reactive oxygen species, toxicity, oxidative stress, and antioxidants: chronic diseases and aging. Archives of Toxicology 97(10), 2499-2574. https://doi.org/10.1007/s00204-023-03562-9.

Kakkar P, Das B, Viswanathan PN. 1984. A modified spectrophotometric assay of superoxide dismutase. Indian Journal of Biochemistry & Biophysics 21(2), 130-132.

Karnam KC, Ellutla M, Bodduluru LN, Kasala ER, Uppulapu SK, Kalyankumarraju M, Lahkar M. 2017. Preventive effect of berberine against DMBA-induced breast cancer in female Sprague Dawley rats. Biomedicine & Pharmacotherapy 92, 207-214. https://doi.org/10.1016/j.biopha.2017.05.069.

Kolanjiappan K, Manoharan S. 2005. Chemopreventive efficacy and anti-lipid peroxidative potential of Jasminum grandiflorum Linn. on 7,12-dimethylbenz(a)anthracene-induced rat mammary carcinogenesis. Fundamental & Clinical Pharmacology 19(6), 687-693. https://doi.org/10.1111/j.1472-8206.2005.00376.x.

Korkmaz E, Tekin S. 2024. Cytotoxicity of myrtenal on different human cancer cell lines. Annals of Medical Research 31(5), 404-408. https://doi.org/10.5455/annalsmedres.2024.04.065

Lakshmi A, Subramanian S. 2014. Chemotherapeutic effect of tangeretin, a polymethoxylated flavone studied in 7, 12-dimethylbenz(a)anthracene induced mammary carcinoma in experimental rats. Biochimie 99, 96-109. https://doi.org/10.1016/j.biochi.2013.11.017.

Lingaiah HB, Natarajan N, Thamaraiselvan R, Srinivasan P, Periyasamy BM. 2013. Myrtenal ameliorates diethylnitrosamine-induced hepatocarcinogenesis through the activation of tumor suppressor protein p53 and regulation of lysosomal and mitochondrial enzymes. Fundamental & Clinical Pharmacology 27(4), 443-54. https://doi.org/10.1111/j.1472-8206.2012.01039.x.

Lokeshkumar B, Sathishkumar V, Nandakumar N, Rengarajan T, Madankumar A, Balasubramanian MP. 2015. Anti-Oxidative Effect of Myrtenal in Prevention and Treatment of Colon Cancer Induced by 1, 2-Dimethyl Hydrazine (DMH) in Experimental Animals. Biomolecules & Therapeutics 5, 471-478. https://doi.org/10.4062/biomolther.2015.039

Lowry OH, Rosebrough NJ, Farr AL, Randall RJ. 1951. Protein measurement with the Folin phenol reagent. Journal of Biological Chemistry 193(1), 265-275.

Mathivadhani P, Shanthi P, Sachdanandam P. 2007. Effect of Semecarpus anacardium Linn. nut extract on mammary and hepatic expression of xenobiotic enzymes in DMBA-induced mammary carcinoma. Environmental Toxicology and Pharmacology 23(3), 328-34. https://doi.org/10.1016/j.etap.2006.12.004.

Obeagu EI, Obeagu GU. 2024. Breast cancer: A review of risk factors and diagnosis. Medicine 103(3), e36905. https://doi.org/10.1097/MD.0000000000036905.

Ohkawa H, Ohishi N, Yagi K. 1979. Assay for lipid peroxides in animal tissues by thiobarbituric acid reaction. Analytical Biochemistry 95(2), 351–358.  https://doi.org/10.1016/0003-2697(79)90738-3

Omaye ST, Turnbull JD, Sauberlich HE. 1979. Selected methods for the determination of ascorbic acid in animal cells, tissues, and fluids. Methods in Enzymology 62, 3-11. https://doi.org/10.1016/0076-6879(79)62181-x.

Omura T, Sato R. 1964. The Carbon Monoxide-Binding Pigment Of Liver Microsomes. I. Evidence For Its Hemoprotein Nature. Journal of Biological Chemistry 239, 2370-2378.

Palan PR, Mikhail MS, Basu J, Romney SL. 1991. Plasma levels of antioxidantβ‐carotene and α‐tocopherol in uterine cervix dysplasias and cancer. Nutrition and Cancer 15(1), 13–20. https://doi.org/10.1080/01635589109514106.

Rotruck JT, Pope AL, Ganther HE, Swanson AB, Hafeman DG, Hoekstra WG. 1973. Selenium: biochemical role as a component of glutathione peroxidase. Science 179(4073), 588-590. https://doi.org/10.1126/science.179.4073.588.

Sinha AK. 1972. Colorimetric assay of catalase. Analytical Biochemistry 47(2), 389-394.

https://doi.org/10.1016/0003-2697(72)90132-7.

Townsend DM, Tew KD. 2003. The role of glutathione-S-transferase in anti-cancer drug resistance. Oncogene 22(47), 7369-7375. https://doi.org/10.1038/sj.onc.1206940

Wali AF, Pillai JR, Talath S, Shivappa P, Sridhar SB, El-Tanani M, Rangraze IR, Mohamed OI, Al Ani NN. 2025. Phytochemicals in Breast Cancer Prevention and Treatment: A Comprehensive Review. Current Issues in Molecular Biology 47(1), 30.  https://doi.org/10.3390/cimb47010030.

Wang Z, Zhang X. 2017. Chemopreventive Activity of Honokiol against 7, 12 – Dimethylbenz[a]anthracene-Induced Mammary Cancer in Female Sprague Dawley Rats. Frontiers in Pharmacology 8, 320. https://doi.org/10.3389/fphar.2017.00320.

Wen H, Yang HJ, An YJ, Kim JM, Lee DH, Jin X, Park SW, Min KJ, Park S. 2013. Enhanced phase II detoxification contributes to beneficial effects of dietary restriction as revealed by multi-platform metabolomics studies. Molecular & Cellular Proteomics 12(3), 575-586. https://doi.org/10.1074/mcp.M112.021352.

Yagi K. 1987. Lipid peroxides and human diseases. Chemistry and Physics of Lipids 45(2-4), 337-351. https://doi.org/10.1016/0009-3084(87)90071-5

Zhang Y, Ji Y, Liu S, Li J, Wu J, Jin Q, Liu X, Duan H, Feng Z, Liu Y, Zhang Y, Lyu Z, Song F, Song F, Yang L, Liu H, Huang Y. 2025. Global burden of female breast cancer: new estimates in 2022, temporal trend and future projections up to 2050 based on the latest release from GLOBOCAN. Journal of the National Cancer Center 1, 287-296. https://doi.org/10.1016/j.jncc.2025.02.002.

Zhang YJ, Gan RY, Li S, Zhou Y, Li AN, Xu DP, Li HB. 2015. Antioxidant Phytochemicals for the Prevention and Treatment of Chronic Diseases. Molecules 20(12), 21138-21156. https://doi.org/10.3390/molecules201219753.

Related Articles

Assessing tree diversity in cashew plantations: Environmental and agronomic determinants in buffer zones of Mont Sangbé National Park, western Côte d’Ivoire

Kouamé Christophe Koffi, Kouakou Hilaire Bohoussou, Serge Cherry Piba, Naomie Ouffoue, Sylvestre Gagbe, Alex Beda, Adama Tondossama, Int. J. Biosci. 27(2), 122-133, August 2025.

Anthelmintic potential of powdered papaya seed Carica papaya in varying levels against Ascaridia galli in broiler chicken

Roniemay P. Sayson, Mylene G. Millapez, Zandro O. Perez, Int. J. Biosci. 27(2), 114-121, August 2025.

Valorization of fish scale waste for the synthesis of functional gelatin-based biopolymers

N. Natarajan Arun Nagendran, B. Balakrishnan Rajalakshmi, C. Chellapandi Balachandran, Jayabalan Viji, Int. J. Biosci. 27(2), 102-113, August 2025.

Isolation and characterization of phosphate solubilising bacteria undernath Excoecaria agallocha L. of muthupet mangrove reserve

Ms. S. Alice Keerthana, V. Shanmugaraju, P. Arun, M. Poongothai, Int. J. Biosci. 27(2), 83-89, August 2025.

Hematological and biochemical parameters in mono- and associative invasions of domestic chickens by helminths and eimeria in Azerbaijan

Aygun A. Azizova, Ramin S. Mammadov, Ugur Uslu, Int. J. Biosci. 27(2), 76-82, August 2025.

Evaluation of phytocompounds from Azima tetracantha using UV-VIS and FTIR analysis

R. Devi Anbarasi, V. Ramamurthy, Int. J. Biosci. 27(2), 69-75, August 2025.